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AAnalyst 600

AAnalyst 600. ES Hwang Inorganic Product Specialist PerkinElmer Korea. Features Dedicated THGA furnace High sensitivity segmented solid-state photodiode detector Simultaneous measurement of sample and reference beams Transversely heated graphite furnace

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AAnalyst 600

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  1. AAnalyst 600 ES Hwang Inorganic Product Specialist PerkinElmer Korea

  2. Features Dedicated THGA furnace High sensitivity segmented solid-state photodiode detector Simultaneous measurement of sample and reference beams Transversely heated graphite furnace Longitudinal Zeeman effect background correction Benefits THGA furnace reduces interferences in difficult matrices Exceptional analytical performance and detection limits Highest Long-term Stability Minimized interferences and memory effects Shorter analysis time (fast furnace programs) Best possible background correction with no light loss AAnalyst 600… … the best dedicated THGA furnace system

  3. AAnalyst 600 AA Spectrometers

  4. AAnalyst 600 Revolutionary Optical System

  5. AAnalyst 600 Unique Features • First AA spectrometer • Integrated furnace • Zeeman-THGA graphite furnace

  6. AAnalyst 600 Unique Features • First AA spectrometer • 8-lamp holder • Automatic lamp selection and adjustment • Built-in power supplies • Hollow cathode lamps • Electrodeless discharge lamps

  7. AAnalyst 600Highly Versatile Furnace Autosampler • User Benefits: • Automatic generation of reference solutions • Automatic multiple injections • Automatic dilution • Automatic injection into a preheated tube • Variable pipetting speed • Ease-of-operation

  8. AAnalyst 600 Revolutionary Optical System • Real time double beam system • High sensitivity segmented solid-state photodiode detector • User Benefits: • Exceptional analytical performance • Highest Long-term Stability

  9. AAnalyst 600 Customized Solid-State Detector • Highest quantum efficiency • Integrated low noise CMOS charge amplifier array • Exceptional signal-to-noise ratio

  10. solid state detector photomultiplier AAnalyst 600 Quantum Efficiency of Detectors

  11. AAnalyst 600 Furnace (THGA) Instrument Detection Limits THGA Instrument detection limits (IDL) / pg Element PMT Photodiode As 9 6 Cr 1.5 0.4 Cu 5 4 Mn 2 1.5 Pb 3 3 Tl 7.5 7

  12. AAnalyst 600 Automatic Lamp Selector • 8-Lamp holder • Built-in power supplies for hollow cathode and electrodeless discharge lamps • Automatic alignment, element, wavelength and slit selection

  13. AAnalyst 600 Unique Overall Conception • Total system control via AA WinLab32 software for highest versatility and simplest operating convenience • Atomizer control • Lamp and lamp current control • THGA control • Accessory control

  14. AAnalyst 600 Unique Software Conception • Automatic system setup from stored user’s methods • Direct from Workspace • Method • Sample information • Individual screen design, window selection etc. • User Benefits: • Analytical reliability • Ease-of-operation • Time-saving

  15. WinLab32 for AA Bringing a new level of productivity to high-performance AA

  16. AA WinLab32 - Features and Benefits • Improve productivity • Data Reprocessing * • WinLab32 Offline * • Priority samples * • Append to Analysis List * • Edit Calibration • Recall Calibration • Furnace Method Development wizard * • Improve ease of use and reduce training • Tool tips (available in 6 languages) * • Wizards * • Analysis List * • AS-93 parameters integrated * * New features not present in 16-bit AA WinLab

  17. AA WinLab32 - Features and Benefits • Reduce training and support • Common look and feel with WinLab32 for ICP-OES • CD Document Pack • Improve stability and data accessibility • Access database * • Method and data security • Password protection * • Multiple user levels * • Data check sums to detect changes * • 21 CFR Part 11 Compliant * New features not present in 16-bit AA WinLab

  18. WinLab32 for AA Workspace Status Monitor Toolbar Automated Analysis Results Calibration Common look and feel with WinLab32 for ICP for easy cross platform training

  19. Data Reprocessing • Recalculation of analytical data • Correct SIF errors • Change calibration function • Delete replicate(s) • Performed using the raw data • Samples can be reprocessed in any sequence • Original data are preserved • Analytical log can be printed • Reprocessed data are identified

  20. Data Reprocessing Status display Select samples in the order you want them reprocessed. Change sample information in these columns

  21. Furnace Method Development Wizard Define Solutions To Analyze Define Furnace Steps to cycle Temperatures Analyze Solutions and Display Results

  22. Align Autosampler Tip Wizard

  23. Auto dilution by system

  24. Priority Sample Samples can be added without interrupting current analyses

  25. Exporting Data to LABWORKS Export data to LABWORKS

  26. WinLab32 Enhanced Security Option • Enhancement to WinLab32 for AA (and ICP) • Significant set of new features • Audit trails • File versioning • Enable compliance with new regulations • 21 CFR Part 11 - Pharmaceutical • 40 CFR Part 3 - Environmental (proposed) • Others • Primarily for highly regulated laboratories • Users actions are restricted • Increased storage space requirements • Additional information entry requirements • Requires more system housekeeping

  27. AAnalyst 600 Total Range Graphite Furnace AA • THGA-type furnace with Zeeman-effect background correction • User Benefits: • Selection of the best system for individual requirements and budgets • High performance, near interference-free trace analysis with STPF concept

  28. AAnalyst 600Integrated THGA Furnace System

  29. AAnalyst 600Zeeman THGA Furnace • Transversely heated graphite furnace • Longitudinal Zeeman effect background correction User Benefits: • Exceptional detection limits • Minimized interferences and memory effects • Best possible background correction • Mimimum sample preparation time • Shorter analysis time (fast furnace programs)

  30. AAnalyst 600 Integrated THGA System • THGA Concept: more than 2500 systems in use • Longitudinal Zeeman-Effect: highly resolved background compensation without light loss • DC furnace power supply • Closest approach to the "ideal system"

  31. AAnalyst 600 Integrated THGA System Atomic and background signals for Ba, 20uL, 25 ug/L

  32. AAnalyst 600Zeeman versus D2 Background Correction • Background correction independent of wavelength • True double-beam with only one optical path • Baseline noise at least 2x lower • Optical resolution Dl is 100x better • Char. mass typically 10 and 20 % poorer than with D2 (the m0 for the worst case, Cu, is 50% poorer) • Zeeman-effect background correction gives superior detection limits in real samples

  33. AAnalyst 600 Highly Versatile Furnace Autosampler • High-capacity, interchangeable sample trays • 88 or 146 sample positions • Full AA WinLab32 control including multi-tasking • User Benefits: • Automatic generation of reference solutions • Automatic multiple injections • Automatic dilution • Automatic injection into a preheated tube • Variable pipetting speed • Ease-of-operation

  34. AAnalyst 600Flow Injection - Furnace Coupling • Optional accessory for coupling FI-MHS with furnace AA • Software controlled automatic operation User Benefits: • Detection limits in range of ng/L • Time-savings by automatic on-line operation • Less interferences since matrix components are removed in the FI system

  35. AAnalyst 600 Automatic Slurry Sampling • Optional ultrasonic probe integrated in the autosampler • Automatic introduction of solid samples as slurries • Full software control User Benefits: • Reduced sample preparation and analysis time • Reduced potential for contamination • Easy operation

  36. What else can PerkinElmer offer? • Sample Preparation Solutions • Multiwave 3000 • High Pressure Asher (HPA) • Flow Injection Technology (FIAS) • For sample pre-treatment • Hydride generation • Stand-alone Mercury systems (FIMS) • Sample Introduction Systems • Autodilutors • Laser Ablation systems • World class service and support

  37. Inorganic sample preparation…. • Multiwave 3000 • Reduced digestion times • Superior digestion quality • Time-saving • Easy operation • Maximum safety • High Pressure Asher • Complete sample mineralization • Minimum organic residue • No elemental losses • No contamination Multiwave 3000 HPA system …a clear solution for sample preparation !

  38. FIAS – Flow Injection Systems • 2 Models • FIAS 100 (1 valve, 1 pump) • FIAS 400 (1 valve, 2 pumps) • Automated sampling for Flame AA • Dilution • Add reagents or modifiers • Matrix removal • Preconcentration • Improved sample handling • Small sample volumes • High solids samples • Hydride generation • Determination of As, Se, Te, Be, Sb, Sn FIAS 100 system FIAS 400 system

  39. Flow Injection Mercury Systems • FIMS 400 • Determines Mercury via Cold Vapor AA (CVAA) • Small footprint • Fully automated • Easy to operate • Stand alone system • Cost effective • Now with WinLab32 for AA software

  40. AAnalyst 600 Conclusions • Not just another AA! • No compromises! • Easiest, simplest AA furnace • Full automation • Full range of accessories • Power of AA WinLab32 software • Ultimate in performance • The AA instrument to take you beyond 2000...

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