Diffractometer - PowerPoint PPT Presentation

X-ray powder diffractometer

X-ray powder diffractometer. film, image plate, or area detector. X-ray powder diffractometer. X-ray diffraction. Braggs' law  = 2d hkl sin  hkl. Debye rings Diameters give  s. film or image paper. X-ray powder diffractometer. rarely used now. X-ray powder diffractometer.

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Example 3.2: PyNinit

Example 3.2: PyNinit Simple structure with non-merohedric twinning. Handling twin overlaps in Jana2006 Single crystal data measured with Oxford Diffraction four-circle diffractometer Input files: 1 st twin domain: pyNinit_twin1.hkl, pyNinit_twin1.sum

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212 views • 8 slides

Example 1: Zn

Example 1: Zn Application of Jana2006 to simple organometallic structure. Creating jobname, reading input files, determination of symmetry, solving structure with charge flipping, editing of atomic parameters, refinement, hydrogen assignment. Chemical formula: (NH 3 CH 2 CH 2 NH 3 ) 2 ZnCl 6

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98 views • 2 slides

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