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Experimental procedure synthesis - PowerPoint PPT Presentation

Experiment 19:

Experiment 19:

Experiment 19:. OXIDATION OF 9-FLUORENOL. Objectives:. To synthesize a ketone from a secondary alcohol using household bleach. To monitor the reaction progress using TLC analysis. To purify product using simple extraction.

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835 views • 20 slides
Experiment 24:

Experiment 24:

Experiment 24:. SYNTHESIS AND GC ANALYSIS OF FATTY ACID METHYL ESTERS. Objectives:. To synthesize fatty acid methyl esters through transesterification of an unknown vegetable oil. To purify your product using column chromatography.

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340 views • 17 slides
Experiment 24:

Experiment 24:

Experiment 24:. SYNTHESIS AND GC ANALYSIS OF FATTY ACID METHYL ESTERS. Objectives:. To synthesize fatty acid methyl esters through transesterification of an unknown vegetable oil. To purify your product using column chromatography.

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279 views • 17 slides
Experiment 20:

Experiment 20:

Experiment 20:. REDUCTION OF 9-FLUORENONE. Objectives:. To synthesize a secondary alcohol from a ketone using a sodium borohydride reduction. To purify and isolate the product using recrystallization. To analyze the purity of the product using TLC, HPLC and melting point analysis.

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3.2k views • 16 slides
Experiment 20

Experiment 20

Experiment 20. SODIUM BOROHYDRIDE REDUCTION OF A KETONE. Objectives:. To synthesize a tertiary alcohol from a ketone using a sodium borohydride reduction. To purify the product using fractional distillation. To analyze the purity of the product using GC.

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466 views • 12 slides

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