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Chemometric in Civil Engineering

Chemometric in Civil Engineering. Kazan State University of Architecture and Engineering. Alfred Suleymanov. The general structure of the University. The University is subdivided in: 1. Institute of Architecture and Design

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Chemometric in Civil Engineering

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  1. Chemometric in Civil Engineering Kazan State University of Architecture and Engineering Alfred Suleymanov

  2. The general structure of the University The University is subdivided in:1. Institute of Architecture and Design      Faculty of General Architectural and Art Training     Architecture Faculty     Design Faculty     Building Design Department     Architectural School for Children DASHKA

  3. The general structure of the University 2 Institute of Transport     Faculty of Transport Engineering      Faculty Engineering Basics 

  4. The general structure of the University 3. Institute of Economy and Building Management     Faculty of Economics     Faculty of Part-time and Extended Studies

  5. The general structure of the University 4. Centre for Humanities Sciences 5. Faculties     Building Science Engineering      Faculty of Engineering Systems and Ecology     Faculty of Construction Technologies      Engineering Faculty for Part-time Studies

  6. Specialties - Architecture - Building Engineering- Restoration and Reconstruction of Architectonical Heritage - Design of Architectonical Environment - Interior Art  - Industrial and Civil Engineering

  7. Specialties - Economy and Business Management - Expertise and Real Estate Management - Heat Supply and Ventilation - Water Supply and Water Removal - Production of Constructional Material, Manufactures and Construction

  8. Specialties - Highway and Airdrome - Transport Organization and Safety - Bridges and Transport Tunnels - Engineering Protection of Environment  - Informational Systems and Technologies - Professional Education (Engineering, Wiring and Repair Technologies)

  9. Scientific directions - Mechanics of deforming solids - Building facilities, edifices and constructions - Heat supply, ventilation, air conditioning, natural gas supply and illumination - Water supply, sewerage systems, building water-preserving systems.

  10. Scientific directions - Building materials and products - Philosophy of science and technology - Theory and history of architecture, restoration and reconstruction of historical-architectural heritage - Architecture of building and constructions. Creative conceptions of architectural activity - City and rural inhabited locality planning

  11. Chemometric techniques in civil engineering • monitoring of historical buildings with non-intrusive measurements (image analysis, acoustic and ultrasonic probing ) • estimation of heterogeneity in concrete slabs, identification of the substrate defects on painted slates, etc. (novel methods of texture analysis);

  12. Chemometric techniques in civil engineering • ecological analysis of pollution; (PCA, PLS and N-way methods) • analysis of aging and degradation of various materials (multivariate projection methods) • quantitative structure – property relationship (QSPR)

  13. Pneumatic and awningconstructions (textile architecture)

  14. Structure of Composite 1-textile reinforcing basis 2-film covering (matrix)

  15. Problems of prediction of polymer materials durability • Degradation processes take place at various structural levels with manifestation of various relationships of cause and effect • Nowadays there is no general theory of polymer aging and destruction • Traditional kinetic approach fails in description of the complicated aging phenomena including both chemical and physical ways of degradation

  16. Problems of prediction … • The situation is even more aggravated with multi-dimensionality and multi-criteriality Under such circumstances we are forced to apply the soft models for prediction of polymer materials durability!

  17. Choice and substantiation of aging parameters (data for construction of mathematical model) • Developing the practical methods for durability prediction it is necessary to choose such characteristics that clearly represent the relationships between the structural changes and material quality • Certainly, it would be nice to get these characteristics without complex methods of structural analysis • Basically, it is impossible to single out a parameter that unequivocally represents both physical and chemical processes in polymeric materials at their aging

  18. Physic-mechanical properties are measured and used for investigation • Durabilityσ and elongation at break ε • The initial module of elasticityЕ • Creep at ageing Δ • ColorΔΕ • Shine • Transparencyα • Limiting wetting angleθ

  19. Colorimetric system CIE Lab

  20. The following aging conditions were simulated • UV sun radiation • Rain • Temperature • Tensile stress

  21. Climatic chambers for experimental researches

  22. Climatic chambers for experimental researches

  23. PVC films before and after ageing

  24. Mechanical properties

  25. Image properties

  26. Durability and Image correlations

  27. Orange pigment at aging

  28. Blue pigment at aging

  29. Blue pigment at aging

  30. PCA Loadings

  31. PCA Scores

  32. PLS Model Predictor matrixX Response matrixY PLS

  33. Tensile strength prediction Calibration set Test set

  34. Elongation at break prediction Calibration set Test set

  35. Green Color Prediction

  36. Regression coefficientsBw

  37. Conclusions Multivariate approach enables us to analyze jointly the material properties in the course of its aging The presented approach substitutes the mechanical testing by a rapid and non-destructive measurement of such physical properties as color, shine and others

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