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ERT 416/3 SYNTHESIS AND PROCESS DESIGN

ERT 416/3 SYNTHESIS AND PROCESS DESIGN. MISS. RAHIMAH BINTI OTHMAN (Email: rahimah@unimap.edu.my). COURSE OUTCOME 1 CO1) CHAPTER 7 : Upstream Processing In Bioprocess Plant. (Week 12) CHAPTER 8 : Bioreaction Design In Bioprocess Plant. (Week 12)

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ERT 416/3 SYNTHESIS AND PROCESS DESIGN

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  1. ERT 416/3SYNTHESIS AND PROCESS DESIGN MISS. RAHIMAH BINTI OTHMAN (Email: rahimah@unimap.edu.my)

  2. COURSE OUTCOME 1 CO1) CHAPTER 7 : Upstream Processing In Bioprocess Plant. (Week 12) CHAPTER 8 : Bioreaction Design In Bioprocess Plant. (Week 12) CHAPTER 9 : Downstream Processing In Bioprocess Plant. (Week 13) [SUBMISSION 2 DESIGN REPORT] - [MIDTERM TEST 2 ] CHAPTER 10: Integrated Bioseparation Scheme for Product Isolation, Purification and Formulation Units For Bioprocess. (Week 14) [SUBMISSION 3 DESIGN REPORT] ORAL PRESENTATION. (Week 15-16)

  3. ERT 416/3SYNTHESIS AND PROCESS DESIGN SUBMISSION 2 & 3 Miss. Rahimah Bt. Othman Email: rahimah@unimap.edu.my

  4. OVERALL DESIGN PROJECT REPORT SUBMISSION 2 : *Chapter 3 - Integration of Energy Process. SUBMISSION 2 : *Chapter 4 - Process Design of Equipment. SUBMISSION 2 : * Chapter 5 - Mechanical Design of Equipment. 5. APPENDIX * AUTOCAD drawings. OUTLINES

  5. OVERALL DESIGN PROJECT REPORT

  6. SUBMISSION 1 • Chapter 1: Literature Review and Process Background. INTRODUCTION OF DESIGN CONCEPT PHYSICAL AND CHEMICAL PROPERTIES PRODUCTION AND MARKETING ANALYSIS DEMAND PLANT SITE LOCATION DESIGN CONCEPTS CONTROL SYSTEM AND EQUIPMENT OVERVIEW PROFITABILITY STUDY ECONOMICAL LOAD ANALYSIS ENVIRONMENTAL IMPACT ANALYSIS RISK ANALYSIS

  7. SUBMISSION 1 • Chapter 2: Design Simulation and Process Flow Diagram. PROCESS FLOW DIAGRAM DESIGN PROCESS BY USING ASPEN HYSYS OR SUPER PRO DESIGN

  8. SUBMISSION 2 • Chapter 3: Integration of Energy Process. Determination of the minimum requirements of heating and cooling in the selected plant system. Selection of the chosen process principles for the integration energy system. Determination process flow conditions. Pinch Temperature Analysis. - (Recommendation: Hint Software) Determination of the minimum number of heat exchanger required. Heat exchanger sizing.

  9. PENYEPADUAN TENAGA CHEW LING NIEN(A81658)

  10. Maklumat Aliran

  11. Rajah Jeram dan Suhu Jepitan

  12. Rajah Suhu-Entalpi dan Komposit Raya Rajah Suhu-entalpi Rajah Komposit Raya

  13. Reka Bentuk Rangkaian Penukar Haba Bertenaga Minimum

  14. Rajah tersepadu

  15. RAJAH ALIR PROSES SELEPAS PENYEPADUAN

  16. SUBMISSION 2 • Chapter 4: Process Design of Equipment. List of all equipment chosen in PFD and justification of the equipment chosen. Preparation of the complete equipment list for the selected process route including the references for all information and data. (The data can be taken from the simulation process plant). Specific process sizing calculation for all equipments by referring to the process conditions of the plant.

  17. SUBMISSION 2 • Chapter 5: Mechanical Design of Equipment. List of all equipment chosen in PFD and justification of the equipment chosen. Preparation of the complete equipment list for the chosen process route including the references for all information and data. (The data are based on process sizing calculation and the simulation process plant) Specific mechanical sizing calculation on the selected equipment by measuring certain plant condition.

  18. SUBMISSION 2 APPENDIX - AUTOCAD drawing for all equipments. * based on process and mechanical sizing parameters. [Chapter 4 : Process Design of Equipment] [Chapter 5 : Mechanical Design of Equipment]

  19. REKA BENTUK REAKTOR

  20. RekabentukProsesReaktorTiub Dan Kelompang DaripadaHysis, Isipadureaktor, VR = 8.958 m3 Panjangtiub, L = 16.886 m Diameter luartiub, do= 0.0822 m (3.2362 in) Diameter dalamtiub, di = 0.0722 m (2.8425 in) Tebaldindingtiub, t = 0.005 m (0.1969 in) N = 100 Kelegaan antara kelompang dan berkas, δ=0.0893 m Diameter dalamkelompang, Ds = 1.4183 m Jarak antara tiub, Pt= 102.75 mm

  21. Mangkin Kromia-alumina, Cr2O3/Al2O3 Keliangan, ε = 0.5 Kesferaan mangkin, ψ= 1 Diameter zarah mangkin, dsf= 1 mm

  22. Kejatuhan Tekanan Pada Tiub Dan Kelompang Kejatuhan tekanan pada sisi tiub, ΔPi = 87.92 kPa Jumlah kejatuhan tekanan sisi kelompang, ΔPs = 5273.63 kPa

  23. RekabentukMekanik Keluli tahan karat 18Cr/8Ni21/2Mo (316) Tebaldinding minimum reaktor = 19.5 mm Ketebalan dinding kelompang, tsebenar = 9 mm (0.35 inci) Tebal minimum tiub yang diperlukan = 4.02 mm Rekabentukkepalaberbentukelipsoid, Ketebalan minimum, th =8.74 mm (0.34 in)

  24. Penyokong Jenis penyokong = Skirt lurus berbentuk silinder Bahan binaan penyokong = Keluli karbon Tinggi penyokong = 2 m Tebal penyokong = 9 mm Gelang Tapak dan Bolt Sauh Jenis bolt = M48 Bilangan bolt diperlukan = 8 Tebal gelang tapak = 20 mm

  25. Bebibir Jenis bebibir = Bebibir kimpalan-leher kelas 150Ib keluli Bahan binaan bebibir = Keluli karbon Jumlah bukaan bebibir = 4 bibibir kimpalan leher Sesekat Potongan sesekat yang digunakan, Bc = 25% Jarak antara sesekat, lB = 425.52 mm Bilangan sesekat yang diperlukan = 40 Ketebalan sesekat = 18 mm

  26. RAJAH REKABENTUK REAKTOR

  27. REKA BENTUK MEKANIK MENARA PENYULINGAN

  28. REKA BENTUK PROSES TURUS PENYULINGAN • Suhu Embun, Tembun = 424.55K • Suhu gelembung, Tbuih= 386.30 K • Nisbah refluks, R = 7.4802 • Bilangan plat sebenar, N = 82.86 ≈ 83 • Diameter Menara = 1.5 m • Tinggi menara,Hv = 57.45 m • Prekabentuk = 2215.932 kPa

  29. REKA BENTUK MEKANIK TURUS PENYULINGAN 1 • Bahagian silinder menara • Bahan binaan = Keluli karbon • Tebal dinding = 0.0156078 m • Penutup • Jenis penutup = elipsoid • Bahan binaan penutup = Keluli karbon • Tebal dinding penutup = 0.0156078 m

  30. Sambungan… • Plat • Jenis plat = Plat katrij • Bahan binaan plat = Keluli karbon • Tebal plat = 2 mm • Diameter lubang tebukan = 5 mm • Bilangan lubang = 6840 • Penyokong • Jenis penyokong = Skirt lurus berbentuk silinder • Bahan binaan penyokong = Keluli karbon • Tinggi penyokong = 2 mm • Tebal penyokong = 15.6078 mm

  31. Sambungan…. • Gelang Tapak dan Bolt Sauh • Jenis bolt = M64 • Bilangan bolt diperlukan = 8 • Tebal gelang tapak = 76 mm Bebibir • Jenis bebibir = Bebibir kimpalan leher dan bebibir buta • Bahan binaan bebibir = Keluli karbon • Jumlah bukaan bebibir = 5 bibibir kimpalan leher, 1 bebibir buta

  32. RAJAH REKABENTUK MEKANIK MENARA PROPENA

  33. SUBMISSION 2 VALIDATION Stamp verification : from PPK Bioprocess Office. Peer assessment form : - last criteria part need to be filled by supervisor. 3. Compulsory to submit design report together with “Peer evaluation form”.

  34. PEER EVALUATION • This mark will be encountered in Sub 1, 2, 3.

  35. GRADING SCHEME

  36. Thank you Prepared by, MISS RAHIMAH OTHMAN

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