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GC setup

GC setup. 2 ml/min. 2 ml/min. 2 ml/min. 103 ml/min. 28 ml/min. 28 ml/min. 24 ml/min. 25 ml/min. 100 ml/min. Split ratio 25:1. Split ratio 24:2. Split ratio 100:1. 2 ml/min. 1 ml/min. 1 ml/min. SPLIT Injections. www.kinesis-solutions.co.uk/kinesis_techtips.asp?id=11.

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GC setup

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  1. GC setup

  2. 2 ml/min 2 ml/min 2 ml/min 103 ml/min 28 ml/min 28 ml/min 24 ml/min 25 ml/min 100 ml/min Split ratio 25:1 Split ratio 24:2 Split ratio 100:1 2 ml/min 1 ml/min 1 ml/min SPLIT Injections www.kinesis-solutions.co.uk/kinesis_techtips.asp?id=11

  3. SPLIT Injections

  4. Peak overload www.chem.agilent.com/cag/cabu/capgccols.htm

  5. 2 mL/min 2 mL/min 3 mL/min 5 mL/min 1 mL/min 3 mL/min SPLITLESS Injections X www.kinesis-solutions.co.uk/kinesis_techtips.asp?id=11

  6. SPLITLESS Injections

  7. DIRECT Injections

  8. Stationary phase interaction

  9. Types of Stationary phases

  10. Temperature Program

  11. Temperature Program

  12. Retention Factor Describes the strength of the interaction of a compound with the stationary phase tR-tM VR-VM k’ = = tM VM 1 < k’ < 10

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