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Mass Spectrometry Fault finding and trouble shooting

Mass Spectrometry Fault finding and trouble shooting

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Mass Spectrometry Fault finding and trouble shooting

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  1. Mass SpectrometryFault finding and trouble shooting Or: Giving the bullet to those pesky faults

  2. Disclaimer Mass spectrometers can cause pain Hot soldering irons can burn 3000 volts can kill 230 Volts can kill Please beware that any work on the instrument is carried out at your own risk. Isomass Scientific cannot be held responsible for injury or damage caused by following these techniques. Protect your eyes Mental pain!

  3. Salesman’s view of solving instrument problems New!

  4. Reality • Budget shortfalls • Not enough money to buy a new instrument • Not enough money to pay for service

  5. What to do • Learn how to look after your own instrument • Go on the manufactures training courses • Ask questions during the installation and any visit made by an engineer • Regularly attend ASITA • Read the manual and other books • Take an electronics course

  6. Fault Finding • Use the instrument supplier as a resource • The engineers are trained on the instrument • The engineers want to help • The engineers will have access to more information • Take your time • Fault finding is not a race • More intervention usually leads to more damage • Take notes and pictures

  7. Fault Finding • Beware of dangerous voltages that might be present in the unit under investigation • The 230 volt supply into most units can be fatal if touched • Source supplies are usually at high voltage, > 3kv • Be careful when connecting or disconnecting meter probes • A badly placed probe can cause a short and further damage • Double check connections and meter setting before turning on the unit under test

  8. Fault Finding • Check power supplies first • Fuses, check with a meter on resistance not just visually • If a supply voltage is less than expected it could be that the supply is damaged or the load is pulling the supply voltage down • Regulated supplies should have very low a.c. ripple • All electronics can be seen as either a supply or load

  9. Fault Finding Think before acting #1 5 minutes thought can save hours of work

  10. Fault Finding Think before acting #2 Think about the problem before acting

  11. Art is a science • Learn to draw • Draw a block diagram of the fault area • Write down the inputs and outputs of each block • Make a list of possible causes

  12. My block diagram

  13. Power Block Diagram

  14. A few simple techniques • Swap • Exchange the suspected part • Measure • Compared the measured parameter with the expected value • Observe • Look to see what’s happening • Write • Keep good notes

  15. Swap Pirani reads atmosphere Pirani reads 1e-3mbar

  16. Simplify Use a blank at point 'A' to test the sub- system within the instrument as a whole Pirani showing atmosphere after 10 minutes pumping

  17. Voltage Measurement

  18. Voltage Measurement • Multimeter set to a.c. or d.c. voltage as required • Black lead in common socket • Red lead in V socket • Voltage measured across one component measures across all components in parallel • Voltage is measured in parallel • Circuit is powered • Connect red probe to one lead of the component and the black probe to the second lead • If meter is auto-ranging note the displayed multiplier

  19. Current Measurement

  20. Current Measurement • Multimeter set to a.c. or d.c. current as required • Black lead in common socket • Red lead in mA or A socket as required, if in doubt start in A socket • Multimeter must be in series with the component • If necessary unsolder one lead from the board • Circuit is powered • Connect red probe to the lead of the component and the black probe to the point the lead was previously connected to • If meter is auto-ranging note the displayed multiplier • Often easier to measure voltage across a resister and use V=IR

  21. Resistance Measurement

  22. Resistance Measurement • Multimeter set to resistance • Black lead in common socket • Red lead in Ω socket • Component must be measured in isolation • Circuit is not powered • If necessary unsolder one lead from the board • Connect red probe to one lead of the resistor and the black probe to the other lead • If meter is auto-ranging note the displayed multiplier

  23. Start with the obvious If a light does not work.... Check the light bulb before dismantling the light switch, changing the fuse in the basement etc.

  24. Start with the obvious If two light bulbs do not work.... Two bulbs might have blown but it's more likely that there is a fault common to both e.g. the fuse in the basement

  25. Fault Finding Take good, clear notes when the instrument is working correctly and notes during any fault finding procedure Don't forget, "RTFM" !

  26. Power Control 230 Volts Control Relay Switched outlet

  27. Vacuum control

  28. Vacuum parts

  29. Vacuum Start-up

  30. Quick Rotary Pump Test

  31. Penning Gauge

  32. Turbo Pump Faults

  33. Vacuum Service • Rotary pump • Change the pump oil every 6 months • Turbo pump • Change the oil wicks yearly

  34. Ion Source Control

  35. Ion Source Electronics ~4.2A 1.5mA ~4A ~700µA ~800µA

  36. Ion source

  37. Exploded Ion Source

  38. Source Cleaning

  39. Magnet Supply

  40. Magnet Screwdriver Test

  41. Inlets

  42. Dual Inlet Valve Control

  43. GC Combustion

  44. EA

  45. GasBench

  46. GasBench

  47. #140, 5700 – 1 Street S.W., Calgary, Alberta T2H 3A9 isomass@isomass.com Tel: (403) 255-6631 . Fax: (403) 255-6958 Toll Free: 1-800-363-7823