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Recent Developments in Polarized Solid Targets. H. Dutz, S. Goertz Physics Institute, University Bonn J. Heckmann, C. Hess, W. Meyer, E. Radke, G. Reicherz Institute for Experimental Physics, Ruhr-University Bochum. Contents: Luminosities of experiments with polarized targets
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Recent Developments in Polarized Solid Targets H. Dutz, S. Goertz Physics Institute, University Bonn J. Heckmann, C. Hess, W. Meyer, E. Radke, G. Reicherz Institute for Experimental Physics, Ruhr-University Bochum
Contents: • Luminosities of experiments with polarized targets • The quality factor of a polarized target: The Figure of Merit • Polarized target Basics: Concept and components • The DNP process • The idea of spin temperatures • The role of the electron spin resonance line • The problem of polarizing deuterons • Three examples for an optimized preparation • The special challange of a large solid angle experiment • Developments concerning internal superconducting magnets • Summary
Polarized Luminosities in Different Beams Lunpol = 1036 – 1037 cm-2s-1 Polarized Solid Targets: Frozen Spin Mode in dilution fridges: up to 107 1/s Continuous Mode in dilution fridges: up to 1 nA Continuous Mode in 4He- evaporators: up to 100 nA Gas Targets: Compressed 3He for external experiments: up to 30 mA H, D storage cells for internal experiments: up to 50 mA COMPASS E155 CB-ELSA < 100nA E154,3He L = 1036 cm-2s-1 < 30mA 1034 1032 1030 1028 HERMES 3He HERMES H,D < 50mA
The Figure of Merit in Asymmetry Experiments - transverse target asymmetry in the case of spin-1/2 - H-Butanol: H H H H H - C – C – C – C –OH H H H H f=10/74~13.5% Measured counting rate asymmetry: Physics asymmetry for a pure target: Dilution factor: = fraction of polarizable nucleons Physics asymmetry for a dilute target: Absolute error of A: small
Measuring time for DA = const : Target Figure of Merit: Typical FoM‘s (continuous polarization at B = 2.5 T, COMPASS like dilution fridge) increasing radiation hardness increasing dilution factors
The Basic Concept of Dynamic Nuclear Polarization Doping and transfer of polarization Cryogenics: 1 K 100 mK NMR: 10 200 MHz Refrigerator Microwaves: 50 200 GHz Magnet: 2 7 T DAQ
The special problem of low m nuclei (e.g. deuterons) DE • Minimize DE while maintaining the thermal contact: DE ~ O(nn) • Find a chemical radical with a narrow EPR line width • Try radiation doping if only low m nuclei present
Example 1: Electron irradiation of 6LiD • Idea: A. Abragam 1980, Saclay • Refinement of preparation: • Since 1991 in Bonn,from 1995 in Bochum COMPASS D • F-Center: • s-wave electron • no g-anisotropy • weak HF interaction + Li 20 MeV at T = 185 K B 7Li (large m) impurity has considerable influence on Pmax 1 liter for COMPASS: Synthesized from highly enriched 6LiD (2000 Bochum) Pmax = 55 % at 2.5 T
Example 3: Trityl doped deuterated alcohols and diols @ B = 2.5 T
CB/ELSA @ Bonn: A 4p double polarization experiment in the frozen spin mode
Disadvantages of the frozen spin mode: • Polarization decays while data taking • Pmax (frozen) ~ 0.8 · Pmax (cont.) • 3) Changing between polarization / measuring modes time consuming and dangerous ! Peff (frozen) ~ 0.7 · Pmax (cont.) • Ways out: • Huge polarizing magnet enclosing the detector • Thin polarizing magnet as part of the refrigerator Already realized as internal holding magnets since middle of 1990 (GDH @ Mainz & Bonn, CB/ELSA) 120mm • Challanges: • High field (B > 2T) with only a few layers 120A current: HT superconductors ! • Mechanical stability of the thin carrier structure Stability of magnet operation • Homogeneous magnetic field (DB/B < 10-4) in a volume comparable to the field volume
Status of the project: Collaboration together with IKP FZ-Jülich and IAM Bonn • Homogeneous volume can not be achieved just by correction coils !!! • Result extremely sensitive to positioning errors of the individual wires • But: Achieveable by a slightly non-cylindrical • shape plus correction coils (DB/B << 10-4 ?) • Theoretical work successfully finished • (patent application) • Test coil to be manufactored in the workshops • of the FZ-Jülich • Internal magnet for transverse polarization: • Saddle coil type with 7 layers • B = 0.5 T @ 30 A • Only problem: Mechanical stability • Order given to a company • Delivery forseen during 2008
Summary: • Due to the limited luminosity a successfull polarization experiment • demands an optimally working polarized target: • Choice of a suitable target material: • Dilution factor • Maximum polarization • Long relaxation times (frozen spin) • Sufficient radiation hardness (more intense beams) • Optimized operating conditions: • Cryostat: Suitable design / high perfomance and reliability • Magnet technology: • Magnets enabling a continuous polarization mode • Magnets for longitudinal AND transverse spin orientation