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Differential (Batch) Distillation

Differential (Batch) Distillation. Bryan Gipson John Usher November 12, 1997. Progress. Familiarization with System 2 Runs Conducted First Run Inconsistent Second Run Okay Data Taken Initial Volume: 14 liters Time vs. Temperature Rate of Distillation. Observations.

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Differential (Batch) Distillation

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  1. Differential (Batch) Distillation Bryan Gipson John Usher November 12, 1997

  2. Progress • Familiarization with System • 2 Runs Conducted • First Run Inconsistent • Second Run Okay • Data Taken • Initial Volume: 14 liters • Time vs. Temperature • Rate of Distillation

  3. Observations • Temperature Change • Less than Predicted • Rate of Distillation • Observed: Sporadic, ~94 ml/min • Theoretical: Decreasing, 215-200 ml/min

  4. Next Steps • Resolve Inconsistencies • Conduct More Data Runs • Estimate Heat Losses • Compare Column Performance to Predictions

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