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XIC of +MRM (7 pairs): 262.2/113.2 amu Max. 5910.0 cps. 3.62 5910 4000 Intensity, cps 2000 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 Time, min XIC of +MRM (7 pairs): 262.2/96.1 amu Max. 2824.0 cps. Ribavirin 3.61 2824 2000 Intensity, cps 1000 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 Time, min XIC of +MRM (7 pairs): 245.1/113.2 amu Max. 962.5 cps. 3.60 963 500 Intensity, cps 3.10 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 Time, min XIC of +MRM (7 pairs): 282.2/150.1 amu Max. 4.2e4 cps. 3.82 Internal standard 4.0e4 Intensity, cps 2.0e4 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 Time, min A Figure 1

XIC of +MRM (5 pairs): 245.2/113.1 amu Max. 5200.0 cps. 5000 4000 Ribavirin 3000 Intensity, cps 2000 1000 0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0 7.5 8.0 8.5 9.0 Time, min XIC of +MRM (5 pairs): 245.2/96.0 amu Max. 305.8 cps. 300 250 200 150 Intensity, cps 100 50 0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0 7.5 8.0 8.5 9.0 Time, min XIC of +MRM (5 pairs): 258.1/126.1 amu Max. 9285.8 cps. 9286 8000 6000 Internal standard Intensity, cps 4000 2000 0 0.5 1.0 1.5 2.0 2.5 3.0 3.5 4.0 4.5 5.0 5.5 6.0 6.5 7.0 7.5 8.0 8.5 9.0 Time, min B Figure 1 (continued)

Internal standard Ribavirin C Figure 1 (continued)

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